2230788-64-2 - Names and Identifiers
2230788-64-2 - Physico-chemical Properties
2230788-64-2 - Introduction
(1 ′-biphenyl)[2-(2 ′-amino-1,1 ′-biphenyl)]palladium(II) methanesulfonate is an organometallic compound. The following is a description of the properties, uses, preparation and safety information of the compound:
Nature:
-Chemical formula: C34H34N2OPS2Pd
-Molecular weight: 692.92g/mol
-Appearance: Light yellow solid
-Melting point: 140-150°C (decomposition)
-Solubility: Soluble in some organic solvents such as dichloromethane, benzene and ethanol
Use:
(1 ′-biphenyl)[2-(2 ′-amino-1,1 ′-biphenyl)]palladium(II) methanesulfonate is an important catalyst commonly used in organic synthesis reactions and has the following applications:
-Catalytic coupling reaction: coupling reaction with organic halides to generate carbon-carbon bonds, commonly used in the synthesis of organic molecular compounds.
-Hydrogenation reaction: In the presence of hydrogen, catalytic hydrogenation reaction reduces the double bond to a single bond.
-reduction reaction: catalytic reduction reaction, such as the reduction of nitroso to amine.
Preparation Method:
(1 ′-biphenyl)[2-(2 ′-amino-1,1 ′-biphenyl)]palladium(II) methanesulfonate can be synthesized by the following steps:
1. [2-(Dicyclohexylphosphino) biphenyl](2 '-amino -1,1'-biphenyl-2-yl) palladium (II) is reacted with methanesulfonic acid in an appropriate solvent.
2. Crystallize, filter and dry the product.
Safety Information:
(1 ′-biphenyl possible)[2-(2 ′-amino-1,1 ′-biphenyl)]palladium(II) methanesulfonate has limited safety data, but based on its chemical structure, has the following safety precautions:
-This compound may be harmful to humans, may cause irritation and damage to the eyes, skin and respiratory system.
-During use, strictly follow laboratory safety procedures and wear appropriate protective equipment, such as gloves, glasses and protective clothing.
-Avoid inhalation, ingestion or contact with skin during operation.
-Avoid contact with oxidizing agents, acids or alkalis during storage and handling.
-In case of accidental spills or breathing difficulties, leave the site as soon as possible and seek medical attention.
Last Update:2024-04-10 22:29:15